Amorphous SiO_2 is prepared by Sol-gel process with chemical reagents of ethal silicate and alcohol, distilled water. Experiments on the phase transformation characteristics of amorphous SiO_2 during heating are conducted by means of TG-DTA and XRD methods. 以正硅酸乙脂试剂、乙醇试剂及蒸馏水为原料,运用溶胶&凝胶工艺制备了无定形纯SiO2,采用TG-DTA、XRD等方法研究了SiO2在加热晶体化过程中的相变特性。