In this reaction, acyl isothiocyanates is employed as raw materials in order to achieve coexistence of many functional groups and provide a new synthesis method of diallyl alcohol or dipropargyl alcohol. 有机卤化锌试剂对酰基异硫氰酸酯的加成反应,可实现多种官能团的共存,提供了一种合成双烯丙基醇和双炔丙基醇的新方法。